Research on Chemical Properties of Pyrolysis Products of Gentamicin Residue

Jia Meng-meng; Li Yi-fei; Feng Li-hui; Wang Zhi-qiang; Ma Si-Lu; Yang Jian; Hu Jia-shuo

doi:doi:10.11648/j.sd.20170506.21

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Research on Chemical Properties of Pyrolysis Products of Gentamicin Residue

Jia Meng-meng, Li Yi-fei, Feng Li-hui, Wang Zhi-qiang, Ma Si-Lu, Yang Jian, Hu Jia-shuo

Published in Science Discovery (Volume 5, Issue 6)

Received: 16 November 2017 Published: 21 November 2017

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Abstract

This paper selected gentamicin ferment residue in the tube furnace reactor for rapid pyrolysis experiments, the ferment residue and pyrolysis products (coke, tar) were analyzed by XPS, FTIR and GC-MS. FTIR analysis showed that the ferment residue and pyrolysis products mainly contain saturated alkanes and proteins, sugars and lipids. XPS results show that the pyrolytic coke is mainly C-C chemical bond, its content increased significantly from 55.07% to 72.27%, while the C-N bond from 18.21% to 5.8%. The chemical constituents of the pyrolysis oil were separated and identified by GC-MS. The identified materials could be divided into: aromatic hydrocarbons, phenol and its derivatives, esters, ketones, acids, amines, nitriles and some heterocyclic compounds; The effect of the pyrolysis temperature on the main components of pyrolysis oil was studied. It was found that the effect of temperature on the composition of the components was not significant, but the relative content of the components was significant. At the same time, the nitrogen-containing compounds in the pyrolysis oil are pyrrole, nitriles and indole, and the content is 9.93% -29.17%.

Published in	Science Discovery (Volume 5, Issue 6)
DOI	10.11648/j.sd.20170506.21
Page(s)	457-462
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2017. Published by Science Publishing Group

Keywords

Gentamicin Ferment Residue, Pyrolysis, XPS, FTIR, GC-MS

References

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APA Style

Jia Meng-meng, Li Yi-fei, Feng Li-hui, Wang Zhi-qiang, Ma Si-Lu, et al. (2017). Research on Chemical Properties of Pyrolysis Products of Gentamicin Residue. Science Discovery, 5(6), 457-462. https://doi.org/10.11648/j.sd.20170506.21

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ACS Style

Jia Meng-meng; Li Yi-fei; Feng Li-hui; Wang Zhi-qiang; Ma Si-Lu, et al. Research on Chemical Properties of Pyrolysis Products of Gentamicin Residue. Sci. Discov. 2017, 5(6), 457-462. doi: 10.11648/j.sd.20170506.21

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AMA Style

Jia Meng-meng, Li Yi-fei, Feng Li-hui, Wang Zhi-qiang, Ma Si-Lu, et al. Research on Chemical Properties of Pyrolysis Products of Gentamicin Residue. Sci Discov. 2017;5(6):457-462. doi: 10.11648/j.sd.20170506.21

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@article{10.11648/j.sd.20170506.21,
  author = {Jia Meng-meng and Li Yi-fei and Feng Li-hui and Wang Zhi-qiang and Ma Si-Lu and Yang Jian and Hu Jia-shuo},
  title = {Research on Chemical Properties of Pyrolysis Products of Gentamicin Residue},
  journal = {Science Discovery},
  volume = {5},
  number = {6},
  pages = {457-462},
  doi = {10.11648/j.sd.20170506.21},
  url = {https://doi.org/10.11648/j.sd.20170506.21},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.sd.20170506.21},
  abstract = {This paper selected gentamicin ferment residue in the tube furnace reactor for rapid pyrolysis experiments, the ferment residue and pyrolysis products (coke, tar) were analyzed by XPS, FTIR and GC-MS. FTIR analysis showed that the ferment residue and pyrolysis products mainly contain saturated alkanes and proteins, sugars and lipids. XPS results show that the pyrolytic coke is mainly C-C chemical bond, its content increased significantly from 55.07% to 72.27%, while the C-N bond from 18.21% to 5.8%. The chemical constituents of the pyrolysis oil were separated and identified by GC-MS. The identified materials could be divided into: aromatic hydrocarbons, phenol and its derivatives, esters, ketones, acids, amines, nitriles and some heterocyclic compounds; The effect of the pyrolysis temperature on the main components of pyrolysis oil was studied. It was found that the effect of temperature on the composition of the components was not significant, but the relative content of the components was significant. At the same time, the nitrogen-containing compounds in the pyrolysis oil are pyrrole, nitriles and indole, and the content is 9.93% -29.17%.},
 year = {2017}
}

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TY  - JOUR
T1  - Research on Chemical Properties of Pyrolysis Products of Gentamicin Residue
AU  - Jia Meng-meng
AU  - Li Yi-fei
AU  - Feng Li-hui
AU  - Wang Zhi-qiang
AU  - Ma Si-Lu
AU  - Yang Jian
AU  - Hu Jia-shuo
Y1  - 2017/11/21
PY  - 2017
N1  - https://doi.org/10.11648/j.sd.20170506.21
DO  - 10.11648/j.sd.20170506.21
T2  - Science Discovery
JF  - Science Discovery
JO  - Science Discovery
SP  - 457
EP  - 462
PB  - Science Publishing Group
SN  - 2331-0650
UR  - https://doi.org/10.11648/j.sd.20170506.21
AB  - This paper selected gentamicin ferment residue in the tube furnace reactor for rapid pyrolysis experiments, the ferment residue and pyrolysis products (coke, tar) were analyzed by XPS, FTIR and GC-MS. FTIR analysis showed that the ferment residue and pyrolysis products mainly contain saturated alkanes and proteins, sugars and lipids. XPS results show that the pyrolytic coke is mainly C-C chemical bond, its content increased significantly from 55.07% to 72.27%, while the C-N bond from 18.21% to 5.8%. The chemical constituents of the pyrolysis oil were separated and identified by GC-MS. The identified materials could be divided into: aromatic hydrocarbons, phenol and its derivatives, esters, ketones, acids, amines, nitriles and some heterocyclic compounds; The effect of the pyrolysis temperature on the main components of pyrolysis oil was studied. It was found that the effect of temperature on the composition of the components was not significant, but the relative content of the components was significant. At the same time, the nitrogen-containing compounds in the pyrolysis oil are pyrrole, nitriles and indole, and the content is 9.93% -29.17%.
VL  - 5
IS  - 6
ER  -

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Author Information

Jia Meng-meng

School of Energy and Environmental Engineering, University of Science and Technology Beijing, Beijing, China
Li Yi-fei

School of Energy and Environmental Engineering, University of Science and Technology Beijing, Beijing, China
Feng Li-hui

School of Energy and Environmental Engineering, University of Science and Technology Beijing, Beijing, China
Wang Zhi-qiang

School of Energy and Environmental Engineering, University of Science and Technology Beijing, Beijing, China
Ma Si-Lu

School of Energy and Environmental Engineering, University of Science and Technology Beijing, Beijing, China
Yang Jian

School of Energy and Environmental Engineering, University of Science and Technology Beijing, Beijing, China
Hu Jia-shuo

School of Energy and Environmental Engineering, University of Science and Technology Beijing, Beijing, China

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APA Style

Jia Meng-meng, Li Yi-fei, Feng Li-hui, Wang Zhi-qiang, Ma Si-Lu, et al. (2017). Research on Chemical Properties of Pyrolysis Products of Gentamicin Residue. Science Discovery, 5(6), 457-462. https://doi.org/10.11648/j.sd.20170506.21

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ACS Style

Jia Meng-meng; Li Yi-fei; Feng Li-hui; Wang Zhi-qiang; Ma Si-Lu, et al. Research on Chemical Properties of Pyrolysis Products of Gentamicin Residue. Sci. Discov. 2017, 5(6), 457-462. doi: 10.11648/j.sd.20170506.21

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AMA Style

Jia Meng-meng, Li Yi-fei, Feng Li-hui, Wang Zhi-qiang, Ma Si-Lu, et al. Research on Chemical Properties of Pyrolysis Products of Gentamicin Residue. Sci Discov. 2017;5(6):457-462. doi: 10.11648/j.sd.20170506.21

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@article{10.11648/j.sd.20170506.21,
  author = {Jia Meng-meng and Li Yi-fei and Feng Li-hui and Wang Zhi-qiang and Ma Si-Lu and Yang Jian and Hu Jia-shuo},
  title = {Research on Chemical Properties of Pyrolysis Products of Gentamicin Residue},
  journal = {Science Discovery},
  volume = {5},
  number = {6},
  pages = {457-462},
  doi = {10.11648/j.sd.20170506.21},
  url = {https://doi.org/10.11648/j.sd.20170506.21},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.sd.20170506.21},
  abstract = {This paper selected gentamicin ferment residue in the tube furnace reactor for rapid pyrolysis experiments, the ferment residue and pyrolysis products (coke, tar) were analyzed by XPS, FTIR and GC-MS. FTIR analysis showed that the ferment residue and pyrolysis products mainly contain saturated alkanes and proteins, sugars and lipids. XPS results show that the pyrolytic coke is mainly C-C chemical bond, its content increased significantly from 55.07% to 72.27%, while the C-N bond from 18.21% to 5.8%. The chemical constituents of the pyrolysis oil were separated and identified by GC-MS. The identified materials could be divided into: aromatic hydrocarbons, phenol and its derivatives, esters, ketones, acids, amines, nitriles and some heterocyclic compounds; The effect of the pyrolysis temperature on the main components of pyrolysis oil was studied. It was found that the effect of temperature on the composition of the components was not significant, but the relative content of the components was significant. At the same time, the nitrogen-containing compounds in the pyrolysis oil are pyrrole, nitriles and indole, and the content is 9.93% -29.17%.},
 year = {2017}
}

Copy | Download

TY  - JOUR
T1  - Research on Chemical Properties of Pyrolysis Products of Gentamicin Residue
AU  - Jia Meng-meng
AU  - Li Yi-fei
AU  - Feng Li-hui
AU  - Wang Zhi-qiang
AU  - Ma Si-Lu
AU  - Yang Jian
AU  - Hu Jia-shuo
Y1  - 2017/11/21
PY  - 2017
N1  - https://doi.org/10.11648/j.sd.20170506.21
DO  - 10.11648/j.sd.20170506.21
T2  - Science Discovery
JF  - Science Discovery
JO  - Science Discovery
SP  - 457
EP  - 462
PB  - Science Publishing Group
SN  - 2331-0650
UR  - https://doi.org/10.11648/j.sd.20170506.21
AB  - This paper selected gentamicin ferment residue in the tube furnace reactor for rapid pyrolysis experiments, the ferment residue and pyrolysis products (coke, tar) were analyzed by XPS, FTIR and GC-MS. FTIR analysis showed that the ferment residue and pyrolysis products mainly contain saturated alkanes and proteins, sugars and lipids. XPS results show that the pyrolytic coke is mainly C-C chemical bond, its content increased significantly from 55.07% to 72.27%, while the C-N bond from 18.21% to 5.8%. The chemical constituents of the pyrolysis oil were separated and identified by GC-MS. The identified materials could be divided into: aromatic hydrocarbons, phenol and its derivatives, esters, ketones, acids, amines, nitriles and some heterocyclic compounds; The effect of the pyrolysis temperature on the main components of pyrolysis oil was studied. It was found that the effect of temperature on the composition of the components was not significant, but the relative content of the components was significant. At the same time, the nitrogen-containing compounds in the pyrolysis oil are pyrrole, nitriles and indole, and the content is 9.93% -29.17%.
VL  - 5
IS  - 6
ER  -

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